By Yong Wang and Jamelyn D. Holladay (Eds.)
ISBN-10: 0841220328
ISBN-13: 9780841220324
ISBN-10: 0841239231
ISBN-13: 9780841239234
Microreaction expertise, with its remarkable warmth and mass move merits in addition to uniform place of abode time and circulate development, is likely one of the few applied sciences with strength to advance effective, environmentally benign, and compact strategies. Novel fabrication and processing thoughts, apparatus, and operational equipment are leading to staggering advancements that transcend "traditional" chemical engineering. those new advancements promise advancements in approach vegetation, and bring about the transformation of our proposal of chemical vegetation into compact, secure, energy-efficient, and environmentally sustainable methods. Microsystems at the moment are on hand in lots of units for advertisement functions together with: micromixers and microreactors as substitute to batch creation in pharmaceutical and high-quality chemical undefined, lab-on-chip units, microsensors, complex fast throughput chemical and catalyst screening instruments (e.g. combi), dispensed or moveable energy and chemical construction, disbursed heating and cooling, or even out of this international functions with NASA. a large variety of topics are mentioned during this e-book starting from catalysis to gas processing to combinatorial concepts to separations to novel reactors all of that are enabled via microtechnology ideas. international well known pioneers (Klavs Jensen, Volker Hessel, Jennifer Holmgren, and Galip Akay) offer bills on either historic advancements and the present state-of-the-art in addition to insights into destiny study and improvement in microreactor and method intensification. examine and advancements are offered by means of undefined, universities, U.S. nationwide Laboratories, and different laboratories situated within the usa and during the international. it really is composed of peer-reviewed chapters from either contributing and invited authors. The overview and unique examine issues contain (1) introductory and normal overviews, (2) microreactors- together with catalysts for microreactors, gasoline processors, milli-second touch time catalysis, fuel to liquid know-how, and biomass conversion; and (3) technique intensification equivalent to micro mixers, reactive membranes, and intensification of separation operations.
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Sample text
Gasoline Vaporization In the second year of the automotive fie1 processing program, emphasis shifted from methanol to gasoline vaporization. Stainless steel rather than aluminum was used to create a robust product and minimize potential corrosion concerns. In addition, sealing challenges with the gaskets necessitated a new approach. Concurrent with this development effort, other researchers at PNNL had used laminate formation and diffusion bonding to create two-stream heat exchangers. This concept was extended to a multi-layered reactor device.
Even more surprising at first sight, former catalytic processes can be carried out without catalyst or co-additive in micro channels, because the respective species can be generated directly at the large specific interface by surface reactions. Examples are the base-he Swuki coupling (5, 74) and the acid-free esterification of a pyrene butyric acid (75). Novel processes can also include a change from cryogenic to ambient temperaturetureprocessing, involving a temperaturechange of more than 70 K, like for the synthesis of phenyl boronic acid (20).
Mono-modal spherical particles of titania with narrow size distribution were successfully produced without precipitation of the particles at the wall. The particle size could be controlled in the range from 40 nm to 150 nm simply by changing the diameter of the inner tube at a low l"MP concentration. 1 inner tube fluid +- outer tube fluid 878,607,307 capillary tube glass tube 3000 All scales in Vrn Fig. 4 Scheme of the dual-pipe reactor and SEMphotographs of the titania particles, produced with drfmnt inner tube diameter, (a) 3 0 7 ~ - I .
Microreactor Technology and Process Intensification by Yong Wang and Jamelyn D. Holladay (Eds.)
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